Patent • #US8895337B1. A top-down method of fabricating vertically aligned Group III-V micro- and nanowires uses a two-step etch process that adds a selective anisotropic wet etch after an initial plasma etch to remove the dry etch damage while enabling micro/nanowires with straight and smooth faceted sidewalls and controllable diameters independent of...
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Method of forming through substrate vias (TSVs) and singulating and releasing die having the TSVs from a mechanical support substrate
Patent • #US8906803B2. Accessing a workpiece object in semiconductor processing is disclosed. The workpiece object includes a mechanical support substrate, a release layer over the mechanical support substrate, and an integrated circuit substrate coupled over the release layer. The integrated circuit substrate includes a device layer having semiconductor devices. The method also...
Method of intrinsic marking
Patent • #US8685599B1. A method of pulsed laser intrinsic marking can provide a unique identifier to detect tampering or counterfeiting.
Method of making a cyanate ester foam
Patent • #US8796346B1. A cyanate ester resin mixture with at least one cyanate ester resin, an isocyanate foaming resin, other co-curatives such as polyol or epoxy compounds, a surfactant, and a catalyst/water can react to form a foaming resin that can be cured at a temperature greater than 50° C. to form...
Method of making a silicon nanowire device
Patent • #US9660026B1. There is provided an electronic device and a method for its manufacture. The device comprises an elongate silicon nanowire less than 0.5 μm in cross-sectional dimensions and having a hexagonal cross-sectional shape due to annealing-induced energy relaxation. The method, in examples, includes thinning the nanowire through iterative oxidation and...
Method of making and ceramic articles with multiple regions of distinct density
Patent • #US8212456B1. A method for producing ceramic articles with multiple distinct regions of density by blending pore formers of different types or amounts with ceramic particles to create multiple pore former/ceramic particle mixtures. The mixtures are placed in a divided die cavity, divider removed and subjected to compaction under pressure to...
Method of making carbon nanotube composite materials
Patent • #US8728566B2. The present invention is a method of making a composite polymeric material by dissolving a vinyl thermoplastic polymer, un-functionalized carbon nanotubes and hydroxylated carbon nanotubes and optionally additives in a solvent to make a solution and removing at least a portion of the solvent after casting onto a substrate...
Method of making nanostructured glass-ceramic waste forms
Patent • #US8772566B2. A waste form for and a method of rendering hazardous materials less dangerous is disclosed that includes fixing the hazardous material in nanopores of a nanoporous material, reacting the trapped hazardous material to render it less volatile/soluble, and vitrifying the nanoporous material containing the less volatile/soluble hazardous material.
Method of making nanostructured glass-ceramic waste forms
Patent • #US8334421B1. A method of rendering hazardous materials less dangerous comprising trapping the hazardous material in nanopores of a nanoporous composite material, reacting the trapped hazardous material to render it less volatile/soluble, sealing the trapped hazardous material, and vitrifying the nanoporous material containing the less volatile/soluble hazardous material.
Method of making photovoltaic cell
Patent • #US9685580B2. A photovoltaic solar cell comprises a nano-patterned substrate layer. A plurality of nano-windows are etched into an intermediate substrate layer to form the nano-patterned substrate layer. The nano-patterned substrate layer is positioned between an n-type semiconductor layer composed of an n-type semiconductor material and a p-type semiconductor layer composed...
Method of making thermally-isolated silicon-based integrated circuits
Patent • #US9824932B1. Thermally isolated devices may be formed by performing a series of etches on a silicon-based substrate. As a result of the series of etches, silicon material may be removed from underneath a region of an integrated circuit (IC). The removal of the silicon material from underneath the IC forms...
Method of manufacturing a fully integrated and encapsulated micro-fabricated vacuum diode
Patent • #US8814622B1. Disclosed is an encapsulated micro-diode and a method for producing same. The method comprises forming a plurality columns in the substrate with a respective tip disposed at a first end of the column, the tip defining a cathode of the diode; disposing a sacrificial oxide layer on the substrate,...
Method of multi-dimensional moment analysis for the characterization of signal peaks
Patent • #US8296078B1. A method of multi-dimensional moment analysis for the characterization of signal peaks can be used to optimize the operation of an analytical system. With a two-dimensional Péclet analysis, the quality and signal fidelity of peaks in a two-dimensional experimental space can be analyzed and scored. This method is particularly...
Method of patterning an aerogel
Patent • #US8226839B1. A method for producing a pattern in an aerogel disposed as a coating on a substrate comprises exposing the aerogel coating to the vapors of a hydrophobic silane compound, masking the aerogel coating with a shadow photomask and irradiating the aerogel coating with ultraviolet (UV) irradiation. The exposure to...
Method of photocatalytic nanotagging
Patent • #US7704489B1. A nanotagged chemical structure comprising a chemical structure with an associated photocatalyst and a tagging nanoparticle (a nanotag) grown in proximity to the photocatalyst, and a method for making the nanotagged chemical structure. The nanoparticle is grown in proximity to the photocatalyst by using a photocatalytic reduction reaction.
Method of producing a direct band gap in indirect band gap materials and light emitting or detecting devices fabricated therefrom
Patent • #US12635299B1. A method for creating direct band gap material from indirect band gap material, the resultant direct band gap material, and corresponding optical devices are described. The method employs atomic layer doping (ALDo) to create closely spaced δ-doped layers, alternating between n-type and p-type dopants, to modify the band structure...
Method of protecting radioactive waste from reaching criticality by using a controller that when contacted by water provides borates that absorb neutrons
Patent • #US12260966B2. A container holds radioactive material. A sub-criticality controller protects the radioactive material from reaching a criticality from contact with the water. The sub-criticality controller includes a metallic composition having at least one metal component and at least one borate component bonded to the at least one metal component. The...
Method of synthesizing tungsten nanoparticles
Patent • #US8372177B1. A method to synthesize tungsten nanoparticles has been developed that enables synthesis of nanometer-scale, monodisperse particles that can be stabilized only by tetrahydrofuran. The method can be used at room temperature, is scalable, and the product concentrated by standard means. Since no additives or stabilizing surfactants are required, this...
Method of tuning physical properties of thermosets
Patent • #US12065562B2. Polymerization-induced phase separation enables fine control over thermoset network morphologies, yielding heterogeneous structures with domain sizes tunable over 1-100 nm. However, the controlled chain-growth polymerization techniques exclusively employed to regulate morphology at these length scales are unsuitable for most thermoset materials typically formed through step-growth mechanisms. By employing binary...
Method to analyze remotely sensed spectral data
Patent • #US7491944B1. A fast and rigorous multivariate curve resolution (MCR) algorithm is applied to remotely sensed spectral data. The algorithm is applicable in the solar-reflective spectral region, comprising the visible to the shortwave infrared (ranging from approximately 0.4 to 2.5 mum), midwave infrared, and thermal emission spectral region, comprising the thermal...
Method to blend separator powders
Patent • #US7303593B1. A method for making a blended powder mixture, whereby two or more powders are mixed in a container with a liquid selected from nitrogen or short-chain alcohols, where at least one of the powders has an angle of repose greater than approximately 50 degrees. The method is useful in...
Method to create gradient index in a polymer
Patent • #US8859190B1. Novel photo-writable and thermally switchable polymeric materials exhibit a refractive index change of Δn≧1.0 when exposed to UV light or heat. For example, lithography can be used to convert a non-conjugated precursor polymer to a conjugated polymer having a higher index-of-refraction. Further, two-photon lithography can be used to pattern...
Method to fabricate functionalized conical nanopores
Patent • #US9387444B2. A pressure-based chemical etch method is used to shape polymer nanopores into cones. By varying the pressure, the pore tip diameter can be controlled, while the pore base diameter is largely unaffected. The method provides an easy, low-cost approach for conically etching high density nanopores.
Method to grow group III-nitrides on copper using passivation layers
Patent • #US8741748B1. Group III-nitride epilayers can be grown directly on copper substrates using intermediate passivation layers. For example, single crystalline c-plane GaN can be grown on Cu (110) substrates with MOCVD. The growth relies on a low temperature AlN passivation layer to isolate any alloying reaction between Ga and Cu.
Method to synthesize lanthanide fluoride materials from lanthanide fluorinated alkoxides
Patent • #US9981893B2. Lanthanide fluorinated alkoxide derivatives can be synthesized from the alcoholysis reaction of the lanthanide bis-trimethylsilyl amide and an excess amount of hexafluoro iso-propanol. Nanoparticles can be formed from the lanthanide fluorinated alkoxide derivatives by a solvothermal or solution precipitation process.
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