Solution-assisted densification of NaSICON ceramics

DWPI Title: Fabrication of dense ceramic for e.g. solid electrolyte, involves adding solvent to powder of sodium super-ionic conductor particles to dissolve particles and applying sintering pressure and sintering temperature to reprecipitate particles
Abstract: A sodium-ion conducting NaSICON ceramic can be densified via the addition of a solvent to a NaSICON powder and subsequent pressing under high pressure and mild heat. Densification to ˜90% relative density can be achieved, providing a path toward low-temperature fabrication of Na-ion conductors.
Use: Fabrication of dense sodium super-ionic conductor ceramic. Uses include but are not limited to solid electrolyte in sodium-ion battery, chemical purification, chemical sensing, and treatment of radioactive waste.
Advantage: The method enables low-temperature fabrication of dense sodium super-ionic conductor ceramic under high pressure and mild heat.
Novelty: Fabrication of dense sodium super-ionic conductor (NaSICON) ceramic involves providing a powder of NaSICON particles, adding a solvent to the powder to partially dissolve the particles in the solvent to obtain a dissolved solution, and applying appropriate sintering pressure and sintering temperature to the dissolved solution to reprecipitate particles.
Filed: 1/20/2021
Application Number: US17153607A
Tech ID: SD 14673.1
This invention was made with Government support under Contract No. DE-NA0003525 awarded by the United States Department of Energy/National Nuclear Security Administration. The Government has certain rights in the invention.
Data from Derwent World Patents Index, provided by Clarivate
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